Winterizing bho with acetone. Winterizing will remove any of the fats/lipids yes.
Winterizing bho with acetone Apr 8, 2015 · I have about two ounces of wax I just blasted, but want to try to winterize this batch. Methanols boiling point is actually 30 degrees less than ethanol. Feb 5, 2014 · When winterizing bho with everclear, is the time spent in the freezer relative to the amount run? I am following a video of a guy running a pound of material and feezing for 12 hours. vacuum purge Mar 6, 2018 · 3 Stage Winterization: Warm crude to 30c Fully dissolve crude in 190 proof ethanol 10:1 (1L crude : 10L etoh) Allow mixture to cool to room temperature Filter over a silica slurry bed in a filter funnel Cool solution to 0c Repeat step 4 Take a representative sample of the solution and add dry ice until the solution stops bubbling Repeat step 4 with sample If more solids are filtered out in This video will detail the process of how we extracted and winterized some BHO (Butane Hash/Honey Oil). Apr 5, 2023 · Table of Contents Introduction to Cannabis Extraction Understanding Cannabinoids and Terpenes Criteria for Solvent Selection Detailed Overview of Commo Mar 11, 2013 · Acetone from hardware store; I distill to remove the trace of heavies always present. Mar 28, 2022 · Winterizing & Polishing of BHO Extracts Butane, a popular solvent used in cannabis extraction, makes beautiful concentrates called Butane Honey Oil (BHO). Winterizing also improves how BHO vaporizes. I would pull an MSDS for the specific supplier, and see what they use. The amount of time and precise temperature are variable depending on the solvent and procedure. You can actuall mix straight ethanol and bho for vape pens. I have tried 190 proof eth, pure acetone, and 99% isopropilic for winterize, differences were minimal, acetone was suggested here not long ago. it is a bit more aromatic but evaporates at lower temps. I recently found a place nearby that sells 100% acetone, and was wondering if this would do a I'm going to try winterizing it and then re-filtering and re-purging. With BHO, you have to redissolve it in alcohol anyway to get the wax out Winterizing & Polishing of BHO Extracts Butane, a popular solvent used in cannabis extraction, makes [] May 31, 2018 · Here now is the dried wax shown distributed by estimation into roughly equal portions and loaded into each test tube. Pour in dish to evaporate. In the videos/instructions I've seen, everyone is blasting onto parchment in a Pyrex dish, then putting the parchment under vacuum to Winterizing & Polishing of BHO Extracts Butane, a popular solvent used in cannabis extraction, makes [] We would like to show you a description here but the site won’t allow us. Premix acetone and pentane, then winterize, filter, and purge. Winterize aka cryo freeze butane solution for 2-12 hours (thc will crash out as an oil) 2. The only downside is you will loose all your alcohol. Jan 30, 2020 · What would you say is the best solvent for winterizing oil? How would you rank ethanol, methanol, and acetone as solvents for winterization? Does it even matter which is used if you winterize at -80C? I’ve always used ethanol at -80, but after doing some stuff with acetone recently I’m wondering if it actually works better? Just wanted to check here before I do side by side experiments to Jan 10, 2013 · Hi all my fellow extractors, I am wanting to winterize my bho , is the only way to do it by using 190 proof everclear ? then freezing for 24 hrs , then Sep 9, 2020 · After you do a bho extraction, wash with etoh right away, take that mixture and wash fresh buds of the same strain you extracted in the tube and then do the lost biologist filtering Tek , EXCEPT DO NOT USE FILTER MEDIAS JUST A WINTERIZATION AND A SECOND FILTRATION AFTER. Explore the process, vacuum purging, and how cannabis extractors use BHO. Manufacturers may implement patented and secretive techniques [2]. Methanol from windshield washer fluid, distilled 2x to constant boiling point. 1. Dec 9, 2015 · You can re-winterize, but water stays suspended in alcohols and acetone. So whether you May 30, 2018 · Acetone is likely going to give the best yield because it will pick up the most impurities as well. It has to have the right polarity and all that jazz. First i process the material into BHO, since I dont have a dewaxing sleeve, I winterize my BHO afterwards. BHO concentrates come in various textures such as wax, shatter, budder, sugar, and sauce. I am still trying to figure out if i like thermos soak vs blasting more, but i definitely love winterizing more than extracting / heat purging and vac Mar 21, 2018 · Can anyone please advise or confirm if I am safe using this to winterize my BHO? I am planning on vacuum purging after winterization, probably 20 to 45 minutes at about 125f and -25mmhg. Only possible way of keeping terps with winterizing bho, ime. filter cold mix through coffee filter, remove fats. I have heard of people using acetone, hexane, and some other solvents but I think that takes a greater knowledge of co solvents. Learn about the winterization process in cannabis extraction, its benefits for oil purity, and the equipment needed for effective extraction techniques. CO 2 extraction will pull the highest amount of fats from a plant. Jun 16, 2021 · Imagine winterizing BHO in Ethanol Just use the search. Learn how it’s made and explore its many subtypes. Just Mason jars, coffee filters, and a freezer. Jul 19, 2018 · Hello! I was curious which solvents are best for winterizing darker/goopy BHO. amount of 190 proof Everclear. Also lots of e-juice companies use ethanol in their juices as it is safe for vaping. g, BHO) in a solvent such as isopropanol or ethanol, and chill in a sub-zero freezer. This process helps to create a THC-A (tetrahydrocannabinolic Acid) dominant product. Your asperator should serve you similarly. Why is acetone used for extraction? Why Acetone is a Good Solvent for Extraction Acetone evaporates very quickly and has a low boiling point. Some producers denature by adding an embittering agent, as well as things like methanol, acetone, or Isopropyl. Why is my shatter so dark? Feb 9, 2019 · Can anybody share a winterizing sop for bho? It’s been years since I’ve done this and have better tech now. Dec 8, 2014 · Welcome to the Growery Message Board! You are experiencing a small sample of what the site has to offer. Using commonly found Winterization methods online, we will attempt Apr 28, 2021 · Types of Extraction and the Impact of Winterization Cold ethanol is the optimum extraction method for minimizing fats in extract. So rather than collecting your product and winterising in ethanol or other solvent, I prefer to dump loaded solvent from extraction column into a jacketed spool where it can be held at cryo temps for a few hours then passed through a filter into collection pot. leave outside (its -43 celcius with wind chill tonight) 24- 36 hrs 3. Yes you do need to purge after using any solvent including ethanol (alcohol). I then pour 190 proof everclear (has to be 190 proof or it wont work very good) into the May 18, 2014 · Ethanol is the solvent of choice for winterizing, its chemical properties make it so. I have tried both processes several times, and acetone consistently coagulates much much quicker than ethanol (like hours vs days), and is easier to purge. Coupla days in the fridge, then filter. Jan 21, 2020 · For the best tasting winterized extracts, I would recommend extracting with very cold butane and filtering in-line. If you want to compare more similar solvents, maybe we should consider the common straight-chain alkanes we know and love (propane, butane, pentane, hexane, heptane Jan 11, 2019 · The process consists of two major steps: Winterization: Dissolve crude extract (e. Winterization is an important process in cannabis oil extraction. I ended up using 151proof everclear, strongest available in mi. My question is, how purged does the BHO need to be, before dissolving in ethanol, and is it safe to purge my BHO at a higher temp? Is it safe to purge my bho at a 130’ f, I figured the oil will experience these high temperatures when I’m Jan 28, 2014 · Yeah but look at all the trouble you have to go through with BHO. Jun 5, 2018 · I know ideally I’d be running cold solvent and inline dewaxing… However, I would like to discuss what to do with an impure extract without sending it off to be refined for distillate. Lot easier just to open a bottle and pour some alcohol through the column. For this example I used some flaky yellow stuff I had laying around. The winterization process can be done in two ways: Dec 15, 2020 · Should you winterize BHO? Winterizing will eliminate the majority of remaining butane and remove undesirables like fats, lipids, and waxes, giving you a beautified concentrate that’s vastly more appealing and safer than the original. A “winterization” process with food grade ethanol (95% or higher) can be used to clean and polish your BNO concentrate. Extract colder. Jun 5, 2018 · For a hydrocarbon extraction I like to use the same solvent system the whole way through. I was wondering if other than mixing the crude oil in an ethanol mixture and heating, if there is any other post processing required to remove all remaining butane prior to rotary evaporating? I am currently decarbing on a hotplate until I can May 27, 2013 · Depends on what they denature with. Acetone is also regularly used for solvent fractionation, which is a more precisely controlled form of solvent winterization used for separating individual lipid fractions. Any information would be greatly appreciated ! Oct 31, 2018 · What everyone should know about BHO BHO, or butane hash oil, is one of the most popular cannabis extracts. I have gone through the tutorial on Jun 5, 2018 · I use a chemical duty pump, it can handle all kinds of things. (Not just coffee filters and ball jars) Should I run crude through the spd first or winterize first? Tools on hand: 200 proof etoh Buchner funnel Celite 545 Activated carbon Spd May 1, 2024 · Winterizing BHO with ethanol will remove the residual butane. Thats why you cant just use any alcohol, or even acetone. I'm glad to report it works supremely well, 95% might evaporate slightly faster, but the lower Jul 17, 2019 · Hi Guys! So real quick, I’ve been working with BHO crude for the past 6 months without fail from winterization to distillation. Learn BHO extraction basics, methods, safety tips, and storage guidelines. Sep 14, 2013 · Is it better to fully purge ur bho before winterizing or can you go direct from the heat bath to the everclear? Sep 23, 2013 · From my understanding ethanol isn't the greatest for winterizing bho because it is both polar and non polar. Or just throw it out GroovyOctopusLabs June 16, 2021, 5:44pm 107 Aug 20, 2022 · How do I winterize my BHO? Does winterizing remove butane? Winterizing will eliminate the majority of remaining butane and remove undesirables like fats, lipids, and waxes, giving you a beautified concentrate that’s vastly more appealing and safer than the original. Removing the Ethanol will also then strip some of the terpenes and it is harder to remove than butane. pour off the terpene fraction into a prechilled 2 liter pyrex measuring cup pour that same solution gradually into a Oct 2, 2014 · When you're winterizing BHO aka absolute grade there's very little difference between trim and bud of the same strain as you're left with a very clean product, almost identical potency. I predissolve my oil in acetone, add methanol until it just begins to clump, then add acetone to make it flow freely again. Behind and in the order they are put in the tubes are the solvents to be tested. If your pump is a water stream there is no risk to your pump, plus won’t require a trap. Jan 10, 2013 · Yes, there is a difference between the simple Alkane n-Hexane (normal) and hexanes, which includes aromatic Alkenes. disolve bho in min. I've heard of people wanting to do it with practically any solvent that can dissolve the oils. . They are Hexane, Dichloromethane, Acetone, Ethyl Acetate, Rubbing Alcohol 70/30 iso/water, and Methanol. I’d place the bucket with the Sep 16, 2024 · Butane hash oil (BHO) is a highly efficient method for making dabbable cannabis concentrates, with the extract typically containing up to 90 THC. I will be working with straight BHO and think I have the procedure almost down but defiantly have a few questions before I begin. Hexane is pretty strictly nonpolar by nature. You can purge out the butane at much lower temps than ethanol and if you are going to winterize your rosin, it will be dissolved in ethanol or some other solvent at some point. Jan 10, 2013 · Ok, ended up deciding against the ISO/brine wash, I didn't even get much wax to precipitate in the iso, even in a dry-ice/iso bath. Winterizing ISO, Methanol, and Denatured alcohol extractions: Sep 20, 2019 · Winterization, aka dewaxing, is a vital step in creating a high-purity extract oil. Please login or register to post messages and view our exclusive members-only content. If you're not winterizing the quality difference is due to the contaminants in the leaf. Jan 30, 2012 · Maybe additional moisture but when i have used 99% solvents i didnt get that. Curious if acetone, ethanol, or isopropyl yields different results. I just have to clarify the method I am going to use , make sure its what I want to be doin ,. Personal experience tells me that winterizing with acetone is significantly easier than with ethanol. May 22, 2014 · The other reason ethanol is good is it is safe for human consumption. Winterizing does remove some of the flavor but not all of it in my experience. Winterization is a process that removes waxes and fats from cannabis oil, which helps increase the purity of the product. Oct 4, 2022 · Howdy I usually run methanol for winterizing for my distillate products; but I’ve been asked for some lower grade crude to be made into honey oil, and I’ve noticed that methanol makes the solution quite red, and I can’t really pull the color out without distillation. Jan 16, 2020 · Winterize with acetone only, filter, then add appropriate amount of pentane to assist purge. Using cold alcohol there's virtually no wax picked up so no winterizing required. Plus I have loads of acetone and everclear is $20 a liter here. You can cold boil with your asperator, the idea is you want a pump that won’t be damaged by vapor. Best way to dry your product would be either washing with sodium sulfate or magnesium sulfate and filtering. 4. Does your BHO leave a lot of material on the nail/dabber after? It is it just harsh? If it melts fully and cleanly winterizing won't help. As noted, extracting with -50C butane will minimize the pickup of longer chain molecules and negate the need to winterize. You can extract with Hexanes and winterize with a polar solvent like alcohol, but you can't winterize with a non polar solvent. I have heard about winterizing BHO and was wondering what people's thoughts on it were? I am thinking about trying this out and was wondering for those who have done this would you use 90%+ ISO, 190 proof everclear or denatured alcohol (95% ethanol 5% methanol). Thanks! Share Add a Comment Sort by: Best Open comment sort options Top New Controversial Old Q&A gysterz • Aug 24, 2016 · Today we're going to do a little experimenting with our food-grade BHO run of Silver Kush. Thinking about trying the closed pressurized column method. Temperatures of -20 to -80°Celsius for 24-48 hours are normal [2 If you want a cleaner product with no residuals rather than using pentane , simply add a small portion of water (5mls) to A super saturated solution of acetone/wax and mix thoroughly. Oct 31, 2014 · I finally got my hands on some of the Everclear 190 (thanks to you guys) so though of giving the winterization process a try. Jul 9, 2024 · Learn how to winterize BHO in your extraction lab for clearer, safer cannabis oil that is free from waxes, fats, lipids, and chlorophyll. Jul 13, 2012 · Has anyone tried using acetone for the winterizing solvent? We've been experimenting with it using our lab grade acetone, and the waxes seem to drop out quicker (3-4 hrs in the deep freeze), and evaporating the acetone off is also pretty quick (a couple hours for a zip of oil using vac May 4, 2016 · I read its better than everclear. You'll gain access to additional forums, file attachments, board customizations, encrypted private messages, and much more! Jul 27, 2019 · See our step by step guide on how to winterize rosin. After filtering, the alcohol is evaporated or vacuumed off, to leave a pristine Absolute. IPA can be used but its not the Ideal solvent. BHO extraction will pick up a moderate amount of fats and the cloudiness will increase. Especially since IDE only need 150ml. This is however more time consuming so less Aug 22, 2018 · So I’m crafting cartridges from flower. Make your concentrate last longer and improve THC percentages using this method. Aug 10, 2016 · I've successfully done the thermos soak method of making bho a few times. Found some good tutorials. May 22, 2014 · i tried winterizing a few times and i love it so much that i don't even care that it does not have great taste like my non winterized bho. Regardless of what kind of cannabis concentrate, this May 25, 2014 · So for those who care I just read on another forum of people winterizing with methanol, or acetone. Throw it through crc if needed. Has any one ever winterized with acetone and wat are your thoughts? Nov 15, 2016 · Winterization is a process that removes plant waxes, fats, and lipids from your bho creating a very hard clear amber shatter. Any tips about how much everclear to use (ratio of everclear to g of BHO), I'm thinking a shot per gram?? Leaving the everclear and oil in the freezer for at least 48 hours, then filtering it through 4 coffee filters secured tightly onto a pyrex dish. Learn why it is necessary in the botanicals industry and 4 easy-to-follow process steps. I’ve noticed ethanol isn’t as bad, curious if we May 2, 2020 · Is it better on the lungs? Click to expand Winterizing will remove any of the fats/lipids yes. and is good in leaving the lipids away, plus it costs far less than 190 proof wich is taxed where we are. assuming you probably don't have those, you can dissolve your BHO in a nonpolar first, do a clean water wash or two (saline water if you have chlorophylls) nd Mar 7, 2012 · Here is what a winterizing filter cake looks like, while still wet. My current process for BHO is melting the crude with a hotplate (never measured the temperature of the hot plate - just melted it down) using a 9:1 ratio (99% room temp isopropyl to crude) placing about 1000grams in a 5 gallon bucket. 2. Less fat will be pulled from the plant the more cold it is. It has tendency to dissolve or form solution with both polar and nonpolar compounds. Once all the acetone evaporates, pour off the water, it should contain any residual acetone with minimal terpene and cannaboid loss. Jan 10, 2019 · Hey I have recently figured that the bho shatter Im making into distillate probably does not need to be purged in ovens for 3 days to remove the butane. My friend successfully used 91% ISO in his freezer to winterize a smaller batch, and it did pull some waxes out. I’ve been using everclear but have heard that some people use heptane? I don’t have any equipment. no winterization required. grnpsxsaxhzxeuveoepcndelpcvqfggisvkpczcnwuqbmbkxlehebuzbqcxvqilmkglsbmwa